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Abstract

Structural study of 6-methyl-4-(thiophen-2yl-methylene-amino)-3-thioxo-3,4-dihydro-1,2,4-triazin-5(2H)-one

Author(s): Mohammad Hakimi, Reza Takjoo, Abdoulhossien Massoudi

The title compound was synthesized from the reaction of 4-amino-6-methyl- 3-thioxo-3,4-dihydro-1,2,4-triazin-5(2H)- one (TAMTTO) with thiophene-2-carbaldehyde. The crystal structure was determined by singlecrystal X-ray diffraction. This compound is monoclinic C2/c with the following unit-cell parameters: a =23.135(6)Å, b =6.1108(13)Å, c= 16.378(4)Å, â = 106.805(3)°, Z = 8 and V = 2216.53 Å3. The final R value was 0.0266 for 2246 measured reflections. The triazine and thiophene ring exhibit 60.02º deviation. The inter- and intramolecular interactions give rise to a 3Dnetwork.


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Organic Chemistry: An Indian Journal received 565 citations as per Google Scholar report

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