The solgel processwas successfully prepared Silver/Silica nanocomposites. In this paper, our aim was to develop the silver based nano composites using sol gel method. This work is mainly focused on to study the synthesis of metal composites by sol gel method. We will also observe the morphologies and dimension of silver nitrate doped nano composites are influenced due to alteration in growth parameters such as different composition or thermal treatment. The structure of the sample prepared was studied using X-ray Diffraction (XRD), Energy dispersive X-Ray Spectroscopy (EDS), High Resolution Transmission ElectronMicroscopy (TEM).